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Filter Cleanliness Analysis Service

Filter Cleanliness Analysis Service

Product ID: analytical-service-filter-testing-cleanliness-extraction|Analytical Service

Professional cleanliness analysis services for semiconductor and high-purity chemical process filters. Covers IPA soak testing (GC-MS/NVR) to evaluate organic leaching, and HCl acid extraction testing (ICP-MS) to detect trace metal leaching. Customized dissolution experiments can be conducted based on actual applied chemicals (such as photoresists, acids and bases, solvents), and PPT-level test reports can be provided to help eliminate sources of pollution in the process.

  • IPA soak test with GC-MS/NVR for organic extractables
  • HCl acid extraction with ICP-MS for trace-metal leaching
  • Custom extractions for photoresist, acids/bases and solvents
  • PPT-level trace analysis reports
  • Designed for semiconductor and high-purity process filters
  • Helps pinpoint and eliminate process contamination sources
Cleanliness verification for high-purity process filters
Organic extractables assessment by GC-MS/NVR
Trace-metal leaching detection by ICP-MS
Custom extractions for photoresist, acids/bases, solvents
Process contamination source troubleshooting
Service scope
Quantified cleanliness qualification of filters: organic extractables, metal extractables and particle shedding covered in one workup, with results expressed per device so they compare directly against a manufacturer cleanliness specification or an incoming-inspection limit. New and used cartridges can be submitted side by side to assess degradation and trace contamination sources.
Test method / standard
Three cleanliness axes in parallel: an IPA soak evaluated by GC-MS and NVR for organic extractables; an HCl acid extraction measured by ICP-MS for trace metals; and particle counting for shedding. Extraction conditions can be customised to the chemistry actually in use — photoresist, acids and bases, solvents — so results reflect the real process.
Instrumentation
ICP-MS / ICP-QQQ (detection limit 1 ppt; the common 30 metals plus silicon, boron, sulfur and phosphorus); GC-MS (detection limit 1 ppb – 100 ppb); non-volatile residue (NVR); and DMA-CPC (detection limit ≥ 100 particles/mL, chemistry dependent) for particle shedding.
Sample requirement
The physical filter; submitting an unused and a used cartridge as a pair makes comparison meaningful. Please state cartridge diameter and nominal length (e.g. 10"), which the per-device calculation requires, and the process chemistry in use so custom extraction conditions can be decided.
Deliverables
Three sets of cleanliness data — organic extractables, metal extractables and particle shedding — reported per device (µg/device, mg/device, ng/device) with extraction conditions and detection limits; a side-by-side column is provided when new and used cartridges are submitted together.
Standard lead time
Confirmed with the quotation, based on scope and sample count. Standard flow: requirement received → samples received → joint review → quotation → project start → laboratory testing → report and walkthrough → customer feedback → additional checks → closure; samples are held for one month after closure before disposal.
Regulatory & validation
Cleanliness data is reported per device so it compares directly against a manufacturer specification or an incoming-inspection limit. Selected extended items are run jointly with partner analytical laboratories nationwide; the performing laboratory is stated in the report.

Note: actual compatibility and service life depend on chemical concentration, temperature, flow, differential pressure, upstream contamination load and housing design. Validate under your real process conditions.

Where it fits

This service is quantified cleanliness qualification of a filter: send it when incoming inspection needs a number that compares against the manufacturer specification, or when a yield problem needs the filter ruled in or out as a contamination source. It covers organic extractables, metal extractables and particle shedding in one workup — leave any one out and the investigation keeps a blind spot.

Key characteristics

Three axes run in parallel: an isopropanol soak evaluated by GC-MS and non-volatile residue for organic extractables; a hydrochloric acid extraction measured by ICP-MS / ICP-QQQ (detection limit on the order of 1 ppt, covering the common 30 metals plus silicon, boron, sulfur and phosphorus) for trace metals; and particle shedding measured by DMA-CPC.

Results are reported per device rather than as a concentration alone, and the difference matters. At the same parts-per-billion figure, a 20" cartridge releases twice the absolute amount that a 10" one does, so comparing concentrations compares the wrong thing. Per-device numbers line up directly against a manufacturer cleanliness specification or an incoming-inspection limit.

Extraction conditions can be customised to the chemistry actually in use — photoresist, acids and bases, solvents — so results reflect the real process instead of a laboratory default.

Choosing between options

The line between this and its neighbours is cleanliness versus capability:

ServiceQuestion it answersReporting unit
Filter cleanliness testing (this)How much does this filter release?Per device
Extractables and leachables testingWhat species does this material release into my chemistry?Identification and quantification by species
Cartridge performance testingWhat does it retain, and how long does it last?Retention efficiency, LRV and dirt-holding capacity

Operation & change-out

What to send: the physical filter, and ideally an unused and a used one as a pair so the comparison means something. Please state cartridge diameter and nominal length (10", for example), which the per-device calculation requires, and the process chemistry in use so custom extraction conditions can be decided. Turnaround is confirmed with the quotation from scope and sample count; samples are held for one month after closure.

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Selected extended items are run jointly with partner analytical laboratories nationwide, and the performing laboratory is stated in the report, so an internal or supplier audit can trace every figure back to where it was measured.
What does the cleanliness test cover?
Two directions: an IPA soak test using GC-MS/NVR to assess organic extractables, and an HCl acid extraction test using ICP-MS to detect trace-metal leaching — covering both the organic and metallic aspects of cleanliness.
Can the test be customized to my actual chemicals?
Yes. The service can run custom extraction experiments based on the chemicals you actually use, such as photoresist, acids/bases or solvents, so test conditions mirror your real process and results are more meaningful.
What detection level does the report reach?
We provide PPT (parts-per-trillion) level trace analysis reports that reveal extremely small amounts of metal and organic extractables, helping you precisely trace and eliminate filter-related contamination in high-purity processes.